Organic Chemistry lab

Eight 20.0 mmol of isopentyl alcohol into a 10 ml meliorate bottom flask match magnetic stir sedan Add 2.3 ml of glacial acetic deadly past stir the mixutre Add .15 ml of concentrated sulfuric acid Connect a peeing cooled condenser to the chemical response flask figure out on the alter urine and heat Reduce the heating rate if the reflux family rises to deep down 2cm of the top of the condenser When the reaction time is up add the reaction mixture to cool to nearly room temperature. secrete off the cooling water and remove the condenser with a few drops of water Transfer the reaction mixture to a love cap cartridge remover tube and add 6 ml of aft(prenominal) using some of the after for the change Ash the reaction mix with the after and remove conservatively Pressure may build up in the caped centrifuge tube During the first washables stir the layers until gas exploitation subsides before you cap the centrifuge tube and vent it frequently Try t o remove all of the sedimentary layer after the last washing to minimize the hail of water in the product Dry the crude isopentyl acetate by adding a small amount of anhydrous sodium sulfate conservatively transfer the eloquent to a dry 5ml conical ampoule using a dry filter tip pipette Try not to transfer any drying agent with the liquid M.W b.p d solubility Acetic acid 60.

1 118 1.049 miscible Isopentyl alcohol 88.1 130 0.815 2.7 Isopentyl acetate 130.2 142 0.876 0.25 sul! phuric acid 98.1 290 1.84 miscibleIf you insufficiency to get a full essay, revise it on our website: OrderEssay.net

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